A visceral demonstration of how neglecting concentration control turns a routine synthesis into a violent thermodynamic failure. It serves as a stark reminder that in chemistry, precision is the only barrier between a successful experiment and a hazardous blowout.
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Hydrazine Blow-Out!Added:
So, I was trying to make some hydrazine the other day. I started with super concentrated sodium hydroxide solution, [music] a 22 molar solution to be exact. I pumped it chock-full of chlorine gas [music] from five trichlor tablets.
These are the 3-in guys, mind you.
Then I prepped an 8.5 molar solution of urea. For my gelatin sheet later, I added 5 g in some warm water.
I put it in the freezer for no more than 5 minutes. When it comes time to add it to the chilled bleach, of course it had seized. I stir it in as best as I can.
Just as I add the freezing urea solution, the whole thing froths into a scary mess.
A week of work literally vaporized.
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